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Wednesday, July 22, 2020 | History

1 edition of Anion exchange method for the determination of plutonium in water found in the catalog.

Anion exchange method for the determination of plutonium in water

Anion exchange method for the determination of plutonium in water

single-laboratory evaluation and interlaboratory collaborative study

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  • 37 Currently reading

Published by Environmental Protection Agency, Office of Research and Development, Environmental Monitoring and Support Laboratory, for sale by the National Technical Information Services in Las Vegas, Nev, Springfield, Va .
Written in English

    Subjects:
  • Chemistry, Analytic -- Quantitative,
  • Plutonium

  • Edition Notes

    Statementby C. T. Bishop ... [et al.]
    SeriesInteragency energy-environment research and development program report ; EPA-600/7-78-122, Research reporting series -- EPA-600/7-78-122
    ContributionsBishop, C. T. 1937-, Environmental Monitoring and Support Laboratory (Las Vegas, Nev.)
    The Physical Object
    Paginationix, 67 p. :
    Number of Pages67
    ID Numbers
    Open LibraryOL14184325M

    Black Sea water samples were collected from depths of 10, 60, ,, and m during the Black Sea Expedition on the R/V KNORR in June The concentrations of radio-cesium and plutonium were determined. Plutonium was extracted from sea water by iron hydroxide co-precipitation, anion-exchange chromatography and electrodeposition Cited by: 1. Determination of uranium concentration in water by liquid anion exchange-delayed neutron analysis R. A. Zielinski, D. M. McKown Pages OriginalPaper.

      Measurements of air, soil and water indicate that Pu was released and broadcast into the environment as a result of the triple reactor meltdowns with estimates of . Plutonium by Ceric Sulfate Titration Test Method 3 Plutonium by Diode Array Spectrophotometry 3 Uranium by Arsenazo I Spectrophotometric Test Method 8–10 Thorium by Thorin Spectrophotometric Test Method 11–13 Iron by 1,Phenanthroline Spectrophotometric Test Method 14–16 Iron by 2,2-Bipyridyl Spectrophotometric Test Method 17–

    Anion-exchange polymer filament coating for ultra-trace isotopic analysis of plutonium by thermal ionization mass spectrometry Joseph M. Mannion, Charles R. Shick, Cited by: Choline chloride from Canada: determination of the Commission in investigation no. TA (final) under the Tariff Act of , together with the information obtained in the investigation. (Washington, D.C.: U.S. International Trade Commission, []), by United States International Trade Commission (page images at HathiTrust).


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Anion exchange method for the determination of plutonium in water Download PDF EPUB FB2

APPENDIX 1 TENTATIVE METHOD FOR THE DETERMINATION OF PLUTONIUM AND PLUTONIUM IN WATER (BY A COPRECIPITATION ANION EXCHANGE TECHNIQUE) This appendix is a reprint of a procedure of the same title by Carl T. Bishop, Ralph Brown, Antonia A. Glosby, Charles A. Phillips and Bob Robinson* of Mound Facility in Miamisburg, Ohio The report.

Technical Report: Tentative method for the determination of plutonium and plutonium in water (by a coprecipitation anion exchange technique) Tentative method for the determination of plutonium and plutonium in water (by a coprecipitation anion exchange technique) Full Record.

Get this from a library. Anion exchange method for the determination of plutonium in water: single-laboratory evaluation and interlaboratory collaborative study. [C T Bishop; A A Glosby; R Brown; C A Phillips; Environmental Monitoring and Support Laboratory (Las Vegas, Nev.)].

Get this from a library. Collaborative study of an anion exchange method for the determination of trace plutonium in water. [C T Bishop; A A Glosby; Charles A Phillips; Mound Facility.]. Other experiments reported are: ion exchange studies of rare earths, absorption of uranium from acetate solutions by ion exchange, determination of anion exchangers suitable for work in fused salts, development of a method of focusing electrophoresis, extraction of hydrochloric acid into a third phase with TBP,more».

Rapid dissolution of plutonium in soil by fusion with ammonium hydrogen sulfate followed by plutonium determination by ion exchange and alpha spectrometry M. Yamamoto Journal of Radioanalytical and Nuclear Chemistry Articles 90 (2), Cited by: Determination of uranium isotopes in environmental samples by anion exchange in sulfuric and hydrochloric acid media Article (PDF Available) in Applied Radiation and Isotopes July with Author: Lyubomir Popov.

Plutonium is chemically separated from a 1-L water sample by coprecipitation with ferric hydroxide, anion exchange and electrodeposition. The test method applies to soluble plutonium and to suspended particulate matter containing plutonium. In the latter situation, an acid dissolution step is required to assure that all of the plutonium dissolves.

This practice is an alternative to Practice C for the ion exchange separation in small mass samples (~5 μg of plutonium and up to mg of uranium in 1 mL of solution) of uranium and plutonium from each other and from other impurities for subsequent isotopic abundance and content analysis by thermal ionization mass spectrometry (TIMS).

In addition to being adapted to smaller sample. Glosby, R. Brown, and C. Phillips, "Anion Exchange Method for the Determination of Plutonium in Water: Single-Laboratory Evaluation and Interlaboratory Collaborative Study," U. Environmental Protection Agency Report, EPA/, Las Vegas, NV, A new method of plutonium speciation in large volume of sea water was developed by using adsorption of Pu(IV)-Xylenol Orange chelate and Pu-Arsenazo chelate on XAD-2 resin, respectively.

A radiochemical method for the simultaneous determination of Pu + Pu and Pu in environmental samples has been developed. In the course of the analysis a Pu tracer was used for estimating the chemical yield of plutonium isotopes. After suitable pre-treatment of the sample, the plutonium nuclides in solution were coprecipitated with iron(lll) hydroxide and calcium oxalate and.

Determination of plutonium, uranium and americium/curium isotopes in environmental samples with anion exchange, UTEVA, Sr and DGA resin M.H. Lee 1 Korea Atomic Energy Research Institute, Nuclear Chemistry Research Division, Daejeon,Republik KoreaCited by: 1.

On the anion exchange resin column. The anion exchange resin separation in nitric acid medium was performed as a possible technique for the separation of plutonium from fission products because of its selectivity for plutonium.Cited by: An Analytical Method for Np Using Anion Exchange Separation of Ut Np~ and Pu Using Anion Exchange Separation of Zr, Np, and Nb Using Anion Exchange Separation of Np ati Pu by Anim Bx,change Separation of BP a- Pu by Cation Exchange Separation and Radiochzmical Determination “ofU and Transuranim Elements Using Barium Sulfate The L8+Level.

“Plutonium,” in Nouveau Traite de Chimie Minerale, Paul Pascal, Genl. Vol. xv, “Uranium et Transuraniens” (Masson et Cie, Paris, ) pp “The Complex Compounds of the Transtiranium ElementsJ” A. Gellman. Determination of Plutonium in Urine: The fission track method requires a two-step anion-exchange separation with highly purified reagent acids in a dust-free Standard Test Method for Plutonium in Water, DppAnnual Book of ASTM Standards, Author: R.

Pietrzak, E. Kaplan. The method is coupled with the liquid–liquid extraction stage taking about two days less than would the ion exchange method. A complete analysis takes about 1 week. Talvitie has described a radiochemical method for the determination of plutonium in soil based on chromatography on an anion exchange resin of a 9 M hydrochloric acid extract.

For this reason, the method for determination of plutonium isotopes has been introduced and validated in Radiation Protection Measurements Laboratory (LPD) of the National Centre for Nuclear Research (NCBJ).

In this method the plutonium is isolated from a sample by coprecipitation with phosphates and separated on a AG 1-X2 by: 3. Ion exchange separation of rare earth elements was initiated by Spedding and Powell to separate fission products obtained from nuclear reactors (Spedding et al.

; Powell,). For several years the cation exchange was the primary method used to obtain individual lanthanides(III).Cited by:. C Practice for The Ion Exchange Separation of Ura-nium and Plutonium Prior to Isotopic Analysis C Test Method forPu Isotopic Abundance By Alpha Spectrometry D Practice for Alpha-Particle Spectrometry of Water E Practice for Evaluation of Mass Spectrometers for Quantitative Analysis from a Batch Inlet (Withdrawn )3.ASTM-D - Standard Test Method for Determination of Metal Cyanide Complexes in Wastewater, Surface Water, Groundwater and Drinking Water Using Anion Exchange Chromatography with UV Detection ASTM-D - Standard Test Method for Determination of Nonylphenol, Bisphenol A, p-tert -Octylphenol, Nonylphenol Monoethoxylate and Nonylphenol.Sources of plutonium isotopes to the marine environment are well defined, both spatially and temporally, which makes Pu a potential tracer for oceanic processes.

This paper presents the selection, optimisation and validation of a sample preparation method for the ultra-trace determination of Pu isotopes (Pu and Pu) in marine samples by multi-collector (MC) by: